Laser metal deposition of steel components using machining waste as build material
Gas atomised metal powders are generally used in laser cladding. However, costly new powders prompt the use of machining swarf as an alternative build material. This paper reports on this investigation and establishes its feasibility.
Thermal and microstructural aspects of the laser direct metal deposition of waspaloy
A potential problem in applying the laser direct metal deposition (LDMD) technique to the fabrication of superalloys is the possibility of an inconsistent microstructure and gamma-prime constituency throughout a component. Understanding the causes for these inconsistencies is a crucial step towards eliminating it and facilitating widespread application of the technique. This article uses thermocouple and pyrometric thermal monitoring of the LDMD process and optical metallographic, scanning electron microscope, and electron backscattered diffraction analyses of components built from Waspaloy to correlate LDMD process parameters and final part microstructural characteristics. Temperatures in thin wall structures show a good match to classical Rosenthal heat flow models. The Waspaloy grain morphology and orientation are found to be sensitive to LDMD power and powder mass flow rate parameters, with columnar grains forming preferentially at lower powder mass flow rates. Results cannot be explained purely in te...
The peculiar thermo-structural behavior of the anionic lipid DMPG.
Aqueous dispersions of the anionic phospholipid dimyristoyl phosphatidylglycerol (DMPG), around 100 mM ionic strength, are known to exhibit a thermal behavior similar to that of the largely studied lipid dimyristoyl phosphatidylcholine (DMPC), which undergoes a gel to liquid crystalline phase transition at 23 degrees C, well characterized by differential scanning calorimetry (DSC), and other methods. However, at low ionic strength, DMPG has been shown to present a large gel-fluid transition region, ranging from 18 to 35 degrees C. This intermediate phase is optically transparent and characterized by a continuous change in membrane packing. Structural properties of the DMPG gel-fluid transition region will be discussed, based on results obtained by several techniques: electron spin resonance (ESR) of spin labels at the membrane surface and intercalated at different depths in the bilayer; light scattering; DSC; small angle X-ray scattering (SAXS); and fluorescence spectroscopy of probes in the bilayer.