Mechanical behavior of A356 matrix nanocomposites fabricated using two step mixing via stir casting technique
In this work an investigation of compressive strength and forgeability behavior have been made to explore the effect of SiC nano particles on A356 alloy matrix for the development of A356/SiC nanocomposites using two step mixing through stir casting technique. A356 alloy ingot was selected as a matrix and AFP+SiCn (99.9% pure aluminium fine powder+nano size SiC mechanically forged by using ball mill at 100 rpm for duration of 10 hours) as a reinforcement. Argon gas was used to protect from oxidation during ball milling process. SiC nano particles were varied from 1% to 5% in a step of 1% by weight. In stir casting technique, stirring process was performed at 500±50 rpm for mixing AFP+SiCn in the melt matrix for total stirring period of 10 minutes in two steps. Composites were poured at 680±20° C into the permanent mould. Compressive strength and forgeability tests of fabricated nanocomposites were evaluated by using hydraulic pellet press machine. To analyze the fractured mechanism SEM microstructure was examined. The presence of SiC nano particles were confirmed by EDX spectrum. It was revealed from the results that compressive strength increases with increment of SiC nano particles and found as 603 MPa at 5% SiC nano particles. Whereas forgeability of the nanocomposites were decreased with the increment of SiC nano particles. SEM micrographs showed the ductile fractured mechanism was dominant over the brittle fracture. The main constituents present in the nanocomposites were verified by EDX spectrum.
OF Al-SiC p COMPOSITES THROUGH POWDER Metallurgy Process and Testing Of Properties
Metal matrix composites are the class of composite materials finding vast applications in automotive, aircraft, defense, sports and appliance industries. A horizontal ball mill has been fabricated for milling of aluminum and SiC particles. The change in powder particle morphology during mechanical alloying of Aluminum and SiC powders using horizontal ball mill was studied. Al-SiCp composites with 5 to 30 weight % of SiCp were fabricated using powder metallurgy process. The various properties viz. hardness, density, porosity, compressive strength, indirect tensile strength and surface roughness were measured. The density, porosity, hardness, compressive strength and indirect tensile strength of Al-SiCp composites were found to increase with increase in the wt. % of SiCp from 5 to 30 weight percent. Mechanical alloying of powders resulted in improvement in hardness and compressive strength of Al-SiCp composites with 5 to 30 weight % of SiCp. The microstructure of polished and etched surfaces of powder metal Al-SiCp composite samples was studied using scanning electron microscope.
Phase characterisation of simulated high burn-up UO2 fuel
Abstract To determine the lattice constant variation with burn-up and the oxidation behaviour at high temperatures, simulated UO2-spent fuels with burn-ups up to 200 GWd tM−1 were prepared by cold pressing and sintering and characterised by X-ray diffraction analysis and thermogravimetry. The fcc-lattice parameter of the sintered samples determined at room temperature, showed a continuous decrease with the simulated burn-up. During oxidation the conversion of the simulated fuels to the (U,FP)4O9 and (U,FP)3O8-type phases was strongly delayed when the simulated burn-up exceeded 80 GWd tM−1. Also, at high burn-ups (>100 GWd tM−1), large fractions of the (U,FP)4O9-type phase remained untransformed to (U,FP)3O8 after prolonged exposure to air at 950–1000°C. This suggests a marked widening of the (U,FP)4O9-phase field when the amount of substituted uranium atoms exceeds values of about 8%.