Optimisation of grinding parameters for wheel loading and dressing
Grinding is a finishing process often used to produce desired surface roughness with required precision and quality. The performance of grinding wheel significantly depends on the nature of the wheel, morphology of the abrasive grits and the grinding parameters namely speed, feed and depth of cut. As the wheel is performing its grinding operation, its cutting surface is being loaded with metal particles of the workpiece. This wheel loading also affects the surface finish of the workpiece. Hence monitoring the grinding wheel loading and dressing at proper time intervals becomes mandatory to get the desired surface finish. In the quest of developing a low cost monitoring system, it is good enough to analyse the wheel loading on widely used metal specimens such as mild steel, HCHCr steel and aluminium under optimised cutting conditions using the conventional silicon carbide and aluminium oxide wheels for better evaluation of the results. In this work the grinding parameters are optimised by using ANOVA technique. A full factorial experiment was carried out at 5% level of significance, i.e. at 95% confidence level.
Optimisation of Micro Injection Moulding Process through Design of Experiments
Abstract The paper presents the optimisation of Micro Injection Moulding (MIM) process through Design of Experiments (DoE). MIM is a relatively new technology which is used for the rapid manufacture of micro components. In order to meet the quality and reliability constraints it is important to reduce variability during its operation due to changes in process parameters. In this study, an understanding of the MIM process and consequently its optimisation is carried out by DoE based on six parameters which influence the surface quality, flow length and the aspect ratio. Significant single process parameters and interactions between them were determined through statistical analysis. For the 2-level test, an aspect ratio of 20, 21, and 20 were achieved respectively for Polypropylene (PP), Acrylonitrile-Butadiene-Styrene (ABS) and Polyoxymethylene (POM).
An Ultrasensitive Analytical Method Based on Chemiluminescence Sensing Electrochemical Parallel Catalytic Reaction Event
An ultrasensitive electrochemiluminescence (ECL) method on the combination of electrochemical parallel catalytic reaction and chemiluminesence signal sensing was proposed for improving ECL analytical characteristics using vanadate(V) as a representative. Vanadate(V) could be electrochemically reduced to generate vanadate(II) which could be chemically oxidized by potassium periodate to regenerate vanadate(V) and give parallel catalytic wave effect. Then, the reduced product of potassium periodate could react with butyl-rhodamine B to emit a sensitive chemiluminescence signal. The chemiluminescence intensity was correlative with vanadate(V) concentration. The investigation on the electrochemical reaction rate constant (k0) confirmed that the speed of electrochemical reaction was faster than that of the subsequent chemiluminescence reaction. The possibility of the combination of electrochemical parallel catalytic reaction with chemiluminescence signal sensing was proved. The similar ECL behaviors could be observed at zirconia nanowires-Nafion modified electrode. Because of the separation and enrichment effect of the modified electrode on vanadate(V), the selectivity and sensitivity was further improved greatly. Based on these findings, a new concept on the combination of electrochemical parallel catalytic reaction and chemiluminesence signal sensing was proposed and an ultrasensitive ECL method for the determination of vanadate(V) was developed at zirconia nanowires-Nafion modified electrode. Under the optimum experimental conditions, the ECL intensity was linear with the concentration of vanadate(V) in the range of 2.0×10−12 mol/L–2.0×10−10 mol/L. The detection limit was 8.0×10−13 mol/L, which was more than 6 orders of magnitude lower than that observed by electrochemical current transduction for electrochemical parallel catalytic reaction at zirconia nanowires-Nafion modified electrode.