On the electrodeposition and characterization of niobium from fused fluoride electrolytes
The electrodeposition of niobium from a binary electrolyte consisting of KF and NaF was characterized and compared with that from the ternary electrolyte of LiF, NaF and KF. The deposition experiments were conducted at current densities between 5 and 35 mA cm−2 and electrolyte temperatures between 725 and 800°C. DTA measurements indicated the melting points to be 450 and 710°C for the ternary and binary electrolytes with added K2NbF7; however, it was necessary to operate both electrolytes above 725°C to obtain dense coherent deposits. Coating morphology was described by optical and scanning electron microscopy studies, while coating structure and properties were characterized by X-ray diffraction analysis. In particular, a series of diffraction measurements were reported to describe the changes in the microstructure of the deposited material as a function of the preparation conditions.
Electrochemical study of the anodic dissolution of iron and nickel in the molten LiFNaFKF eutectic at 600°C using convolutional voltammetry
Abstract The kinetics of the anodic dissolution of iron and nickel are studied in the molten LiFNaFKF eutectic at 600°C by voltammetry. In order to eliminate distortion of the voltammograms by ohmic drop, convolutional techniques are used. The standard potentials of both Fe/Fe(II) and Ni/Ni(II) systems are determined by logarithmic analysis of semi-integrals.
Globalization and the Internationalization of Legal Education in the United States: An Annotated Bibliography
Globalization and its influence on legal education is a topic of growing interest to the legal profession and to legal educators alike. The first articles on the subject appeared in the mid-1990s, and the frequency of publications has been increasing ever since. This bibliography provides annotations to English-language law journal articles published between 1995 and 2008 that focus on the impact of globalization on legal education in the United States.