Evaluation of single liquid primers with organic sulfur compound for bonding between indirect composite material and silver-palladium-copper-gold alloy.
The purpose of this study was to evaluate the effect of primers on bonding between a silver-palladium-copper-gold alloy and an indirect composite material. Cast disks were air-abraded with alumina, conditioned with one of five primers (Alloy Primer, Luna-Wing Primer, Metal Primer II, Metaltite, M.L. Primer), and bonded with a light-activated indirect composite. Shear bond strengths were determined after 20,000 times of thermocycling. The results showed that four of the primers, except the Luna-Wing Primer, were effective in enhancing the bond strength as compared with the unprimed control group. Of these four primers, Alloy Primer, Metal Primer II, and M.L. Primer exhibited significantly greater bond strengths. It can be concluded that the effectiveness of primers varies considerably according to the organic sulfur compounds added to the solvent, and that care must be taken in selecting priming agents for bonding the composite material and the silver-palladium-copper-gold alloy.
Shear bond strength of resin composite veneering material to gold alloy with varying metal surface preparations.
STATEMENT OF PROBLEM
Although adequate surface preparation is indispensable to achieve a consistent and durable bond between resin composite materials and the metal substructures of veneered restorations, information on the bonding performance of current metal adhesive systems is limited.


PURPOSE
The purpose of this study was to evaluate the surface preparation effects of 4 metal conditioners and 1 adhesive system on bonding between a prosthetic resin composite veneering material and a gold casting alloy.


MATERIAL AND METHODS
Four primers containing sulfur derivative monomer and designed for conditioning noble metal alloys (Alloy Primer, Infis Opaque Primer, Metal Primer II, and Metaltite) and a surface modification technique (Siloc) were assessed. Cast disk specimens made of gold alloy (Pontor LFC) were either primed with 1 of the 4 primers or treated with the Siloc system and bonded with a light-activated prosthetic resin composite material (New Metacolor Infis). Control specimens were also prepared without the use of a bonding agent. Shear bond strengths were determined before and after thermocycling (20,000 cycles) for evaluation of bond durability.


RESULTS
All of the primed and Siloc-treated groups showed improved 24-hour shear bond strengths compared with the control group. After thermocycling, the groups either primed with the Metaltite conditioner or treated with the Siloc system exhibited the highest mean shear bond strengths.


CONCLUSION
The Metaltite conditioner and Siloc system each represent a useful method for improving the bond between the gold alloy and resin composite material tested.
Tensile bond strengths of composites to a gold-palladium alloy after thermal cycling.
STATEMENT OF PROBLEM
Many different materials and methods have been used to fabricate or repair veneer facings with composites, but only a few of these have been studied.


PURPOSE
This study compared the tensile bond strengths of composites to a gold-palladium alloy with the use of several surface treatment methods.


MATERIAL AND METHODS
Forty alloy specimens were cast in Eclipse (52% gold and 37.5% palladium) in the form of truncated cones. These specimens were divided equally into 4 groups. In group I, the bonding surfaces of the metal cones were treated with Silicoater MD. Truncated cones of Dentacolor composite were bonded to the metal surfaces and light-polymerized. In group II, the bonding surfaces of the metal cones were air-particle abraded with 50 microm aluminum oxide and coated with C&B Metabond. Truncated cones of Epic-TMPT composite were bonded to the metal surfaces and light-polymerized. In group III, the bonding surfaces of the metal cones were air-particle abraded with CoJet-Sand. Truncated cones of Pertac-Hybrid composite were bonded to the metal surfaces and light-polymerized. In group IV, the bonding surfaces of the metal cones were air-particle abraded with CoJet-Sand. Truncated cones of Visio-Gem were bonded to the metal surfaces and light-polymerized. After 24 hours of water immersion at 37 degrees C and 1000 thermal cycles in water at 5 degrees C and 55 degrees C, tensile forces were applied to all specimens with a universal testing machine. Analysis of variance was applied to the data (P<.05), and differences among means were determined with a Tukey-Kramer interval of 5.4 MPa.


RESULTS
Tensile bond strengths in MPa were as follows: Dentacolor, 14 +/- 5; Epic-TMPT, 12 +/- 4; Pertac-Hybrid, 13 +/- 5; and Visio-Gem, 18 +/- 4. The tensile bond strength of Visio-Gem was significantly higher than that of Epic-TMPT, but no differences were found among Dentacolor, Pertac-Hybrid, and Epic-TMPT (P<.05).


CONCLUSION
Within the limitations of this study, all 4 bonding systems tested produced high bond strengths between composites and a gold-palladium alloy after thermal cycling.