Statistical Investigation of Parameters Influence on Fracture Toughness of the Glass Fiber Reinforced Composites
The objective of the work was to investigate statistical analysis of fracture toughness of the glass fiber reinforced composites at different stacking sequences, strain rate and crack length. The glass reinforced vinylester composites prepared by hand layup technique with stacking sequences of 0/90, 45/-45 and chopped strand orientations. 3- point bending for fracture toughness test for various notch depth ratio's as per linear elastic fracture mechanics concept was conducted. Further the initial notch depth method was adopted to find the critical stress intensity factor KIC for the given notch depth ratio. Design of experiment using Taguchi L9 array was formulated to understand the influence of parameters on fracture toughness. The result of surface methodology showed the stacking sequence of (45/- 45/0/90/Chopped)3s, with strain rate of 0.5 mm/min and without notch having the highest fracture toughness of 81.36 Mpa
Fracture mechanisms and failure processes at stiffener run-outs in polymer matrix composite stiffened elements
Abstract This paper describes the fractographic analyses of three stringer run-out designs which had been loaded to failure in tension. The main aims of the investigation were to deduce the failure processes in the elements, and to characterise the effect of local geometry of the stringer run-out on the failure process. The analysis showed that the critical failure mechanism in the elements was the development of +45° ply splitting at the skin surface, initially under mode I dominated intralaminar fracture. However, as these splits grew beneath the stringer foot, the mode II component increased. This led to mixed-mode delamination growth, extending parallel to the +45° ply, at the skin/adhesive interface. Subsequently, the delamination migrated through the skin via ply splits, ultimately reaching the interface between the second and third (−45°/0°) plies, in which it remained until catastrophic failure. Extending and tapering the stringer foot led to shifting of the site of the +45° ply splitting; this was attributed to in-plane tensile stresses in the skin being inhibited in the modified designs. The reduced out-of-plane support on the stiffener foot in the modified designs led to an increase in the mode I component at the delamination from the stringer tip. It also led to an increase in the degree of multi-plane delamination growth. Based on the fractographic observations, recommendations for modelling the elements were suggested.
A bifunctional Cr/Yb/Tm:Ca3Ga2Ge3O12 phosphor with near-infrared long-lasting phosphorescence and upconversion luminescence.
Currently, upconversion nanocrystals and long-lasting phosphorescent particles have attracted extensive research interest for their possible applications as bioimaging probes. However, there are few reports concerning the achievement of both upconversion luminescence of lanthanide ions and long-lasting phosphorescence of transition metal ions in a sole host so far. Herein, we demonstrate a novel calcium gallium germanium garnet (Ca3Ga2Ge3O12) host where lanthanide ions such as Tm(3+)/Yb(3+) and transition metal ions such as Cr(3+) can be easily incorporated through substituting the Ca(2+) and Ga(3+) respectively. This Cr/Yb/Tm:Ca3Ga2Ge3O12 phosphor exhibits both broadband near-infrared long-lasting phosphorescence of Cr(3+) with an afterglow time of more than 7000 s and near-infrared to near-infrared upconversion luminescence of Tm(3+). Impressively, it is evidenced that the addition of Yb(3+)/Tm(3+) into Cr:Ca3Ga2Ge3O12 not only results in Tm(3+) upconversion luminescence but also greatly increases Cr(3+) afterglow time. Based on excitation/emission, three-dimensional thermoluminescence, and time-resolved luminescence spectra, the related long-lasting phosphorescence and upconversion luminescent mechanisms are systematically discussed as well.