Noise diagnostics of advanced composite materials for structural applications
Our study is focused on noise diagnostics of an advanced composite material for structural applications called extren, which consists of a combination of a fibre glass reinforcement and a resin binder. Electromagnetic and acoustic emission signals appear during mechanical loading of the material under investigation. They carry information about micro-cracks generated in tested materials. We made long-time simultaneous multi-channel measurements of both signals for various loading conditions, carried out time development of noise spectrum, evaluated parameters of EME and AE events, studied their time development, correlations between them and made statistical analyses of signals and their parameters.
Experimental study of electromagnetic emission signals generated by crack generation in composite materials
The formation of a crack is accompanied by the generation of an electromagnetic field. A differential equation was derived and solved to describe the transformation of the field parameters into an electric signal, provided capacitive sensors are used. In the next stage, an analysis of spurious external electromagnetic and acoustic fields was carried out, and measures to suppress their effects were designed. The issue of amplifying extremely low electromagnetic signals generated during the crack formation was dealt with, too. The mentioned analyses resulted in the design of a method to detect and evaluate electromagnetic emission (EME) signals and acoustic emission (AE) signals, which accompany mechanical stressing of materials and structures. Based on the results of such analyses, an automated double-channel measuring apparatus was used for signal data acquisition, saving and processing. The operation of the apparatus was successfully tested by processing a large set of measurement results obtained from a composite material called ‘extren’. Our experimental results confirmed the correctness of both the EME and AE measurement methods, and measuring apparatus design. Our measurement results make it possible to track the behaviour of cracks, localize them and evaluate some of their basic parameters.
Thermal incompatibility analysis of metal-ceramic systems based on flexural displacement data.
The feasibility of simple tests or analytical methods for prediction of residual stress states in metal-ceramic (MC) prostheses has not been demonstrated. Biomaterial metal-ceramic strips have been proposed to provide sensitive measures of transient and residual stress states through the measurement of midpoint deflection after cooling from the ceramic sintering temperature. The objective of this study was to apply the elastic-viscoelastic analogy to calculate transient and residual midpoint deflections in MC biomaterial strips and to compare these values with deflections measured with a beam-bending viscometer (BBV). Calculations and measurements were made for five MC systems that were found from a clinical study to be "thermally compatible" systems. Metal strips, 64 mm in length, 3 mm wide, and either 0.5 mm, 1.0 mm, or 2.0 mm in thickness, were veneered with four 0.25-mm thick layers of opaque porcelain. Midpoint deflection of the MC strips (ceramic oriented in the posterior position) was measured during cooling from an initial temperature of 700 degrees C. In general, the directions of the measured residual deflections did not agree with the "textbook" convention that negative deflections are associated with positive thermal contraction mismatch (alpha(M) - alpha(c) > 0) regardless of metal thickness. For a metal thickness of 0.5 mm, the residual midpoint deflection for all thermal contraction mismatch cases, except one, was positive (upward deflection) whereas the residual midpoint deflections were all negative when the metal thickness was increased to 1 or 2 mm, independent of the thermal contraction mismatch. The best agreement between calculated and measured values of residual midpoint deflection (+16 microns vs. +14 +/- 2.3 microns, respectively was obtained for MC biomaterial strips with a Ni-Cr alloy (0.5 mm thick) while the largest difference (+346 microns vs. +61 +/- 43.8 microns) was obtained for MC bimaterial strips with a Au-Pd allow (0.5 mm thick). In all but one case, changes in deflection direction as a function of metal thickness were correctly predicted by the viscoelastic analysis. The results of this study indicate that a viscoelastic model is useful for estimating thermal compatibility conditions of MC systems.