Fabrication of spherical particles with mixed amorphous / crystalline nanostructured cores and insulating oxide shells
By spark-eroding Fe75Si15B10 in water/ethanol mixtures, spherical particles with nanostructured cores consisting of mixed amorphous and crystalline phases were produced. The relative volume fractions of the amorphous and crystalline phases were dependent on the water/ethanol ratio. In the same process, continuous oxide layers were formed on the particle surfaces. The basic mechanisms responsible for the formation of the surface oxide layers and the core nanostructures were modeled. At frequencies ranging from 1 to 100 MHz, the combination of the core nanostructures and the insulating oxide shells yielded exceptionally low-loss magnetic behavior.
Theoretical models of the electrical discharge machining process. I. A simple cathode erosion model
A simple cathode erosion model for the electrical discharge machining (EDM) process is presented. This point heat‐source model differs from previous conduction models in that it accepts power rather than temperature as the boundary condition at the plasma/cathode interface. Optimum pulse times are predicted to within an average of 16% over a two‐decade range after the model is tuned to a single experimental point. A constant fraction of the total power supplied to the gap is transferred to the cathode over a wide range of currents. A universal, dimensionless model is then presented which identifies the key parameters of optimum pulse time factor (g) and erodibility (j) in terms of the thermophysical properties of the cathode material. Compton’s original energy balance for gas discharges is amended for EDM conditions. Here it is believed that the high density of the liquid dielectric causes plasmas of higher energy intensity and pressure than those for gas discharges. These differences of macroscopic diele...
SR topography of plastically deformed Fe-Si bicrystals - observation in situ and post mortem
SR reflection topography was applied to study the interaction of slip dislocations with the grain boundaries in Fe-4at%Si bicrystals deformed by compression. Three experimental settings with either a white or monochromatic beam were used and the corresponding orientation contrast analysed. Dislocation transmission through the grain boundary was observed in bicrystals with favourable geometry of the slip systems.