Determination of impurities in graphite using synchrotron radiation based X-ray fluorescence spectrometry.
Determination of impurities namely Ca, Mn, Fe, Ni, Zn, Sr and Pb in graphite by energy dispersive X-ray fluorescence spectrometry is described using microfocused synchrotron radiation. The internal standard and standard addition methodologies were adopted for quantification and the results were compared with tube-based X-ray fluorescence spectrometry. Analysis of the results by the F and t-tests revealed their statistical equivalence. Synchrotron measurements improved the detection limits by an order of magnitude compared to the tube based technique. Cr and Zr, which were below the quantification limit in tube based technique, were also quantified by synchrotron based technique.
Graphite—the most fascinating nuclear material☆
Abstract A review is made of the behaviour of graphite subjected to irradiation in nuclear reactors with particular emphasis on the dimensional changes of graphite crystallites and their relationship to the macroscopic dimensional changes of polycrystalline graphites. The theory of the formation of the lattice defects responsible for these changes is examined and deficiencies in present knowledge highlighted.
Enumeration of total coliforms, fecal coliforms, and Escherichia coli in foods by hydrophobic grid membrane filter: supplementary report.
Raw, comminuted poultry meat was used to determine the specificity of the media and incubation conditions used in the hydrophobic grid membrane filter method. Confirmation rates for target colonies were 100% for total coliforms, 98% for fecal coliforms, and 97-99% for Escherichia coli. The results of total coliform enumeration in 30 pasteurized milk samples by both the hydrophobic grid membrane filter method and AOAC method 46.013-46.016 are also reported.