Research Summary: Reducing the variations in laser welding
Objective Interactions between lasers and materials are very complex phenomena. The success of laser welding procedures in dental metals depends on the operator's control of many parameters. The aims of this study were to evaluate factors relating to the operator's dexterity and the choice of the welding parameters (power, pulse duration and therefore energy), which are recognized determinants of weld quality.Design In vitro laboratory study.Materials and methods FeNiCr dental drawn wires were chosen for these experiments because their properties are well known. Different diameters of wires were laser welded, then tested in tension and compared to the control material as extruded, in order to evaluate the quality of the welding. Scanning electron microscopy of the fractured zone and micrograph observations perpendicular and parallel to the wire axis were also conducted in order to analyse the depth penetration and the quality of the microstructure. Additionally, the micro-hardness (Vickers type) was measured both in the welded and the heat-affected zones and then compared to the non-welded alloy.Results Adequate combination of energy and pulse duration with the power set in the range between 0.8 to 1 kW appears to improve penetration depth of the laser beam and success of the welding procedure. Operator skill is also an important variable.Conclusion The variation in laser weld quality in dental FeNiCr wires attributable to operator skill can be minimized by optimization of the physical welding parameters.
Optimization of operator and physical parameters for laser welding of dental materials
Objective Interactions between lasers and materials are very complex phenomena. The success of laser welding procedures in dental metals depends on the operator's control of many parameters. The aims of this study were to evaluate factors relating to the operator's dexterity and the choice of the welding parameters (power, pulse duration and therefore energy), which are recognized determinants of weld quality.Design In vitro laboratory study.Materials and methods FeNiCr dental drawn wires were chosen for these experiments because their properties are well known. Different diameters of wires were laser welded, then tested in tension and compared to the control material as extruded, in order to evaluate the quality of the welding. Scanning electron microscopy of the fractured zone and micrograph observations perpendicular and parallel to the wire axis were also conducted in order to analyse the depth penetration and the quality of the microstructure. Additionally, the micro-hardness (Vickers type) was measured both in the welded and the heat-affected zones and then compared to the non-welded alloy.Results Adequate combination of energy and pulse duration with the power set in the range between 0.8 to 1 kW appears to improve penetration depth of the laser beam and success of the welding procedure. Operator skill is also an important variable.Conclusion The variation in laser weld quality in dental FeNiCr wires attributable to operator skill can be minimized by optimization of the physical welding parameters.
Increasing pulp yield in kraft cooking of softwoods by high initial effective alkali concentration (HIEAC) during impregnation leading to decreasing secondary peeling of cellulose
Abstract Pulp yield can be improved by a more homogeneous delignification of the chips, achieved by improved impregnation prior to the cooking stage. Complete and efficient impregnation is obtained by increasing the diffusion rate by means of an impregnation liquor with a high initial effective alkali concentration (HIEAC). In the present study, the effect of HIEAC in the impregnation was evaluated and compared to a reference impregnation procedure and a prolonged impregnation. After the various impregnation scenarios, the alkali concentration was always adjusted to the same level in the beginning of the cooking stage. Impregnation with a HIEAC resulted in yield improvements by 1–1.5% units, due to a higher cellulose yield and possibly also to higher yield of glucomannan. The HIEAC with an even alkali distribution within the chips prior to the cooking stage resulted in a more uniform delignification carbohydrate degradation. Yield increase obtained by uniform delignification is due to both decreased shives content as well as less secondary peeling.