Fractures and rock properties estimated by 3D directional borehole radar
Borehole radar is widely used in civil engineering work such as fault and fracture exploration, salt dome investigation, tunnel detection, UXO detection, exploring locations of foundation piles and sheet metal piling walls, and so on. Borehole radar surveys in resistive rock field have been applied successfully due to the lower attenuation of the rock media. Through those studies, many researchers have become interested in the detectability of thin open fractures and their locations. Though there are some numerical computing studies [1] on its detectability related to the open widths of fractures, there are very few experimental field studies. Thus studies using directional borehole radar system are essentially required at borehole sites where geometrical features and open widths of the fractures are well investigated. We are conducting experimental evaluation surveys for our 3D directional borehole radar system, “ReflexTracker®”. In soft ground in an alluvial plain, a single-hole measurement was carried out to evaluate the detection ability of a conductive cylinder buried 2m from the survey hole and found that the system could detect 3D reflectors representing the target and provided information on the direction of arrival wave and distance to the target [2]. We conducted another experimental measurement to evaluate fracture detectability of the system in rock field. The experimental borehole (BOA-200), a vertical borehole with diameter of 86-115 mm reaching 200 m depth in andesite rock, is located in a rock quarry in Ishikoshi Town, Miyagi Prefecture, Japan. Fractures in the borehole and their geometrical features such as strikes, dips and open widths were investigated in detail by borehole scanner [3], and the electrical characteristics were also obtained by a logging survey for all depths. The radargrams obtained by the non-directional antenna indicate that the arrival times and amplitudes were clearly related to rock mass classification and fracture densities, i.e., the higher the density, the larger the amplitude and the earlier the arrival time. Moreover, interpreted relative permittivities were negatively correlated with resistivities. On the other hand, the interpreted 3D reflectors derived from the directional antenna resulted in significantly good fitting with some of the known fractures' extended planes. Through the experimental study in the rock field, the ReflexTracker shows high potential for applications in fracture extractions and rock property investigations.
Super-resolution of overlapped waves in time and frequency domain in a directional borehole radar measurement
The Multiple Signal Classification (MUSIC) algorithm is modified in order to resolve multiple waves and to estimate reflection points in 3-D space. This algorithm is suitable for directional borehole radar with a circular dipole array antenna. Making use of the spatial frequency difference of acquired array signals, the signals are decorrelated, and the 3-D MUSIC algorithm is applied. The time domain signals of the singlehole array-type borehole radar are used in order to form a measurement vector in the MUSIC algorithm. A computer simulation confirms that the proposed algorithm may estimate the directions of arrival (DOA) for three signals. Applying the proposed algorithm to field experiment data successfully estimates the DOA of a reflected wave from a fracture in rock.
Novel method for the determination of the methoxyl content in lignin by headspace gas chromatography.
The paper reports on a headspace gas chromatographic (HS-GC) method for the determination of methoxyl in lignin. The method involves the quantitive cleavage of methoxyl with hydroiodic acid (HI) to form methyl iodide in a closed headspace sample vial at 130 °C for 30 min. After HI has been added, the sample is neutralized by injecting a sodium hydroxide solution; the methyl iodide in the vial was determined by HS-GC using a flame ionization detector. The results showed that the method has an excellent measurement precision (RSD < 0.69%) and accuracy (RSD < 3.5%) for the quantification of methoxyl content in lignin. The present method is simple and accurate and can be used for the efficient determination of methoxy1 content in lignin and related materials.