Thermal plasma synthesis of SiC from rice hull (husk)
Recently the synthesis of ultrafine powders has drawn considerable attention because these powders can have physical and chemical properties superior to those of bulk specimens. In particular, emphasis is on the preparation of ultrafine ceramic powders for their applications in the development of sintered products having higher density and lower sintering temperature. One such industrially important ceramic material is SiC. In many cases ultrafine SiC has been prepared by thermal plasma processes [1]. However, these processes require one or more reactive/corrosive gases. This letter describes a new method to overcome such problems. For this purpose thermally pretreated rice hull was used as the solid precursor. Rice hull, an agricultural waste product, was first used by Cutler [2] as a starting material for the production of silicon carbide. Since the rice hull route promises to be most economical, much attention has recently been paid to it [3-6]. Rice hull consists of silica in hydrated amorphous form, and cellulose which yields carbon when thermally decomposed. The relative abundance of silica with very high surface area in close proximity to active carbon in rice hull makes it amenable for SiC formation during the pyrolysis process. The possible reaction was given by Lee and Cutler [7] as
High-vacuum synthesis of SiC from rice husk: a novel method
A new technique for the production of SiC from rice husk is reported in this paper. The high-purity β-SiC is synthesized in a short time of 5 min. The samples are characterized by x-ray diffraction and scanning electron microscopy analysis. The results are compared with the previously reported result that was obtained by conventional process.
The National PKI of Peru: a new certification hierarchy
In order to guarantee secure transactions through the Internet and to generate strong evidence that could be used in case of future legal disputes, several countries around the world have promoted and regulated the use of digital signatures based on Public Key Infrastructure (PKI). However, despite the high expectations, its implementation has achieved neither the desired results nor its globalization. Many of the reasons were discovered years ago, but they are still open problems for the scientific community nowadays. In order to consider the case of the national PKI of the Peruvian state as empirical evidence for studies that address the open problems, this article describes the details about a new certification hierarchy which is expected to overcome some of its predecessors’ limitations. It is also expected that the information disclosed in this article could be useful to other countries for making a preliminary assessment for possible cross-border recognition of Peruvian digital signatures.