Fabrication, Mechanical and Dielectric Characterization of 3D Orthogonal Woven Basalt Reinforced Thermoplastic Polyimide Composites
The 3D orthogonal woven basalt fiber reinforced polyimide (PI) composites were fabricated and characterized in this study. The PI film was firstly prepared to determine PI processing parameters. Fourier transform infrared (FTIR) analysis showed that 300°C was the suitable imidization temperature. Thermal gravimetric analysis (TGA) and differential scanning calorimetry (DSC) results showed relatively good thermal properties of the PI film. In the fabrication of composites, the multi-step impregnation method was applied. The bending properties of 3 mm-thick composite showed increasing trend in all and the second-time impregnated composite had much higher value than the first-time impregnated composite. Moreover, the bending fracture mode photos showed obvious creases except for the first-time impregnated materials, which agreed well with the bending property values. The dielectric constants for the composites were complex because they had not regular value following the mixing rule of the composites, which was mainly due to the interfacial polarization and other effects in the fabrication processing.
Evaluation of tribological performance of surface-treated carbon fiber-reinforced thermoplastic polyimide composite
The effect of surface treatment [rare earth solution (RES) and air oxidation] of carbon fibers (CFs) on the mechanical and tribological properties of carbon fiber-reinforced polyimide (CF/PI) composites was comparatively investigated. Experimental results revealed that surface treatment can effectively improve the interfacial adhesion between carbon fiber and PI matrix. Thus, the flexural strength and wear resistance were significantly improved. The RES surface treatment is superior to air oxidation treatment in promoting interfacial adhesion between carbon fiber and PI matrix. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2008
Traceability strategy for gear-pitch-measuring instruments: development and calibration of a multiball artifact
There is a strong demand to ensure the traceability of gear-measuring instruments (GMIs). We propose a multiball artifact (MBA) for the evaluation of pitch-measuring accuracy. The aim of the MBA is to transfer the minimum uncertainty from a calibrated value at the National Metrology Institute of Japan (NMIJ) to a measured value of GMIs at a shop floor. The MBA is composed of equally spaced high-accuracy balls around an axis. The pitch-measuring accuracy of GMIs is evaluated by measuring the angular pitch deviation of the balls instead of the angular pitch deviation of a gear. We calibrated the angular pitch deviation using a coordinate measuring instrument (CMM) at the NMIJ and adapting a multiple-orientation technique. We proposed a calibration strategy of the angular pitch deviation. The calibration value of the pitch deviation for the MBA at the NMIJ was obtained with a measurement uncertainty (U95) of 0.2 µm. We evaluated the pitch-measuring accuracy of a GMI using the calibrated MBA. Each value of U95 for the cumulative and single pitch deviations for the left and right flanks was less than or equal to 0.5 µm. The small uncertainty was transferred from the NMIJ to the GMI.