Inspection and Image Analysis of Nickel Sulphide Inclusions in Toughened Glass Panels
Nickel sulphide is a kind of detrimental inclusion in toughened glass panels. Once the critical conditions are satisfied, the inclusion will cause the shattering of glass panels. An inspection tool was developed for rapid detection of inclusions. More than one thousand pieces of glass were inspected and seventeen of them were found with inclusions. With the experiment of heat soak, and analysis of dispersive energy spectrum, the appearance of nickel sulfide inclusion was presented, which can be used as guidance of in-line inspection of glass panels. The optical system was improved to get clear image of inclusions inside glass panels. Auto focus technique was used to measure the depth of inclusions, which can provide a parameter for the categorization of inclusions
Impedance Spectroscopic Study of Nickel Sulfide Nanostructures Deposited by Aerosol Assisted Chemical Vapor Deposition Technique
This research aims to synthesize the Bis(di-isobutyldithiophosphinato) nickel (II) complex [Ni(iBu2PS2)] to be employed as a substrate for the deposition of nickel sulfide nanostructures, and to investigate its dielectric and impedance characteristics for applications in the electronic industry. Various analytical tools including elemental analysis, mass spectrometry, IR, and TGA were also used to further confirm the successful synthesis of the precursor. NiS nanostructures were grown on the glass substrates by employing an aerosol assisted chemical vapor deposition (AACVD) technique via successful decomposition of the synthesized complex under variable temperature conditions. XRD, SEM, TEM, and EDX methods were well applied to examine resultant nanostructures. Dielectric studies of NiS were carried out at room temperature within the 100 Hz to 5 MHz frequency range. Maxwell-Wagner model gave a complete explanation of the variation of dielectric properties along with frequency. The reason behind high dielectric constant values at low frequency was further endorsed by Koops phenomenological model. The efficient translational hopping and futile reorientation vibration caused the overdue exceptional drift of ac conductivity (σac) along with the rise in frequency. Two relaxation processes caused by grains and grain boundaries were identified from the fitting of a complex impedance plot with an equivalent circuit model (Rg Cg) (Rgb Qgb Cgb). Asymmetry and depression in the semicircle having center present lower than the impedance real axis gave solid justification of dielectric behavior that is non-Debye in nature.
Methods of determining the desired frequency characteristics of the automatic control systems
Considered the methods of determining the desired frequency characteristics of the automatic control systems while the synthesis of their corrective devices.