Comparative measurement of residual stresses with the method based on the magnetic Barkhausen noise and the relaxation method
For an efficient prediction of residual stresses in a material or a machine part the non-destructive method based on the magnetic Barkhausen noise is, among others, employed in practice. An experimental system developed at home and including measuring and assessment units has proved to be very efficient in various applications of surface hardening or cold hardening, and heat treatment.
Residual Stress State Characterization of Machined Components by X-ray Diffraction and Multiparameter Micromagnetic Methods
Machining induced residual stress states have been identified to affect the distortion of parts during following heat treatments. Thus, ideally a complete characterization of the components residual stress state is required. Magnetic and micromagnetic analysis of residual stresses can represent an important gain of time compared to X-ray diffraction. Investigations with these two methods were performed on different components with various and inhomogeneous residual stress states: cylindrical and tapered ball bearing rings made from AISI52100 steel and a disc made from AISI5210 steel. Reliable results and good agreement between X-ray diffraction data and residual stresses obtained from the magnetic and micromagnetic analysis can be obtained with the use of a calibration for each single component. An important gain of time can be achieved with the combined use of X-ray diffraction analysis for the calibration and the micromagnetic technique. However, local residual stress variations in zones smaller than the sensor size may not be detected. A global calibration of the micromagnetic equipment with one calibration file for several parts still needs optimization.
Synthesis of β-FeSi2 nanowires by using silicon nanowire templates
Si nanowires templates were grown by a Cu-catalyzed vapor–liquid–solid process and used for the preparation of β-FeSi2 nanowires on a Si substrate. The silicon nanowires were transformed into β-FeSi2 nanowires by annealing with additional source material containing FeCl2 and Si powder. In contrast to uniform Si nanowire templates along the direction, the synthesized nanowires were deformed irregularly. The electron diffraction pattern of the nanowires synthesized from the template corresponded to that of single-crystalline β-FeSi2 and the longitudinal direction of the nanowire was along the direction. The energy dispersive X-ray fluorescence analysis confirmed that the nanowire contained Fe and Si in an atomic ratio of approximately 1:2. The results confirmed that β-FeSi2 nanowires on a Si substrate were synthesized from the Si nanowire templates.Si nanowires templates were grown by a Cu-catalyzed vapor–liquid–solid process and used for the preparation of β-FeSi2 nanowires on a Si substrate. The silicon nanowires were transformed into β-FeSi2 nanowires by annealing with additional source material containing FeCl2 and Si powder. In contrast to uniform Si nanowire templates along the direction, the synthesized nanowires were deformed irregularly. The electron diffraction pattern of the nanowires synthesized from the template corresponded to that of single-crystalline β-FeSi2 and the longitudinal direction of the nanowire was along the direction. The energy dispersive X-ray fluorescence analysis confirmed that the nanowire contained Fe and Si in an atomic ratio of approximately 1:2. The results confirmed that β-FeSi2 nanowires on a Si substrate were synthesized from the Si nanowire templates.