Investigation of MgF2 optical thin films with ultralow refractive indices prepared from autoclaved sols.
We have successfully developed a process to form high quality MgF(2) thin films with ultralow refractive indices from autoclaved sols prepared from magnesium acetate and hydrofluoric acid. And we have confirmed that our porous MgF(2) coatings have not only high transmittance in the UV region but also high uniformity of film thickness. They can be uniformly formed on phiv 300 mm substrates as a single coating and as a hybrid coating with sublayers formed by physical vapor deposition. They are expected to be applied to various optics that need high transmittance in the UV region.
Investigations of MgF2 Optical Thin Films Prepared from Autoclaved Sol
MgF2 thin films with ultra low refractive indices were obtained by sol–gel method using sols prepared from magnesium acetate and hydrofluoric acid. The sols were autoclaved in a Teflon cell at 100–180°C for 24 h and then coated on SiO2 glass or CaF2 crystal substrates by spin coating. Subsequently, the samples were heat treated at 150°C for 1 h. The optical properties of the thin films, such as refractive index and transmittance, were investigated in the UV region, especially in the deep UV (DUV, below 250 nm) region. Though the coatings consist of single layers, both samples exhibited high transmittance. In addition, they exhibit such antireflection effect over a very wide range of wavelength. Such a good antireflection effect was produced only by low refractive indices. It has also been confirmed that, even in the range of vacuum UV (VUV, 200–150 nm), CaF2 samples with antireflection coatings could keep such a good antireflection effect.
In-House Industrial Production of the Superconducting Conductor for the 43 T Hybrid Magnet of LNCMI-Grenoble
The hybrid magnet being built at LNCMI-Grenoble is based on the combination of resistive inserts, made up of Bitter and polyhelix coils, with a large bore superconducting outsert. It will produce, in the first step, an overall continuous magnetic field of 43 T in a 34 mm warm bore aperture. The superconducting coil will provide a nominal magnetic field of 8.5 T in a 1.1 m cold bore diameter. It relies on the novel development of an Nb-Ti/Cu Rutherford Cable On Conduit Conductor (RCOCC) cooled down to 1.8 K by a bath of superfluid helium pressurized at 1200 mbar. After a brief reminder of the specificity of hybrid magnets, namely the strong electromechanical coupling between resistive and superconducting coils, the main requirements of the RCOCC for efficient and reliable magnet operation are given. The test and validation phases prior to the industrial production of the RCOCC are reported, including the trial production of the ½ hard-drawn (H02 cold-worked) Cu-Ag 0.05% hollow stabilizer in continuous lengths of 325 m. The novelty of the RCOCC development concerns the assembly and the induction soft-soldering of the Rutherford cable on the Cu-Ag hollow stabilizer allowing a strict control of the interstrand contact resistance. Studies, developments, and the integration of the industrial production line at LNCMI-Grenoble are presented together with the result of the production of all RCOCC unit lengths.