Cure Monitoring of Composite Carbon / Epoxy through Electrical Impedance Analysis
Composite materials are increasingly used in aeronautic; they offer many benefits such as mechanical strength, mass and consumption reduction. However, their process development needs to be known and controlled, in order to adjust the process parameters and optimize the characteristics of structures made from these materials. This paper is focused on impedance spectroscopy measurement and analysis technique to characterize material’s properties. In fact, the composites based on carbon fiber have electrical proprieties; therefore a three-dimensional modeling of the electrical conduction in the material is established by using a distributed allocation of an electrical resistance (RP) in parallel with a capacitance (CP). Then, thin electrodes (40 μm thick) are inserted inside the material and a specific impedance measurement bench is developed to perform real-time measurements of RP and CP on unidirectional (UD) mono-ply and multi-plies samples. During curing (in an oven) the change in values of both RP and CP in different stages of the curing cycle is showed. Then, problems that occur during the curing cycle (layup defect, loss of vacuum) were detected by a large gap of the measured electrical parameters in comparison with the ordinary case. Therefore, by this electrical measurement, we present a way to ensure an automated real-time monitoring of the composite curing
Electrical impedance spectroscopy for measuring the impedance response of carbon-fiber-reinforced polymer composite laminates
Abstract Techniques that monitor the change in the electrical properties of materials are promising for both non-destructive testing and structural health monitoring of carbon-fiber-reinforced polymers (CFRPs). However, achieving reliable monitoring using these techniques requires an in-depth understanding of the impedance response of these materials when subjected to an alternating electrical excitation, information that is only partially available in the literature. In this work, we investigate the electrical impedance spectroscopy response at various frequencies of laminates chosen to be representative of classical layups employed in composite structures. We clarify the relationship between the frequency of the electrical current, the conductivity of the surface ply and the probing depth for different CFRP configurations for more efficient electrical signal-based inspections. We also investigate the effect of the amplitude of the input signal.
Scaffolds Containing Spirulina sp. LEB 18 Biomass: Development, Characterization and Evaluation of In Vitro Biodegradation.
Polymer nanofibers are nanomaterials that can be used as scaffolds in tissue engineering. The objective of this study was to develop, characterize and evaluate the in vitro degradation of a biomaterial consisting of nanofibers produced from biodegradable and biocompatible polymers with potential applications as a scaffold for tissue regeneration and containing Spirulina sp. LEB 18 biomass as the bioactive compound. The polymers used were poly(hydroxybutyrate-co-hydroxyvalerate) and polycaprolactone. The polymeric solutions exhibited sufficiently high viscosity to produce uniform nanofibers with diameters between 335 and 617 nm. The applied conditions were as follows: a voltage of 25 kV, a distance from the capillary to the collector of 120 mm, a capillary diameter of 0.80 mm, and 12% polycaprolactone and a blend of 5% polycaprolactone and 10% poly(hydroxybutyrate-co-hydroxyvalerate). The biomass was incorporated into the nanofibers at a concentration of 3%, and the incorporation was confirmed using confocal microscopy. The nanofibers were characterized using differential scanning calorimetry and thermogravimetric analysis, which showed that the addition of biomass did not alter the thermal properties of the biomaterial. The addition of biomass improved the tensile strength and elongation of the scaffolds compared with those produced with polymers alone. A biodegradation assay showed enzymatic action toward the biomaterial, simulating the behavior of natural tissue. Based on the analysis, it was concluded that the scaffolds that were produced have the potential to be applied in the field of tissue regeneration as biomaterials with pharmacological properties.