화합물 132 - E 2 LC / MS ESI 426 ( M + H ) + 1 H NMR ( 500 MHz , MeOD ) δ 7 . 59 ? 7 . 57 ( m , 2 H ) , 7 . 42 ? 7 . 38 ( m , 3 H ) , 7 . 22 ( d , J = 8 . 0 Hz , 1 H ) , 6 . 40 ( d , J = 7 . 5 Hz , 1 H ) , 4 . 33 ( d , 1 H ) , 3 . 46 ? 3 . 30 ( m , 4 H ) , 3 . 16 ? 2 . 93 ( m , 2 H ) , 2 . 72 ( t , J = 6 . 0 Hz , 2 H ) , 2 . 55 ( t , J = 7 . 5 Hz , 2 H ) , 2 . 25 ? 2 . 05 ( m , 2 H ) , 1 . 91 ? 1 . 87 ( m , 2 H ) , 1 . 85 ? 1 . 73 ( m , 2 H ) , 1 . 68 ? 1 . 62 ( m , 2 H ) , 1 . 48 ? 1 . 31 ( m , 4 H ) . 키 랄 SFC A ( 40 % MeOH ) : ee 98 %, Rt = 3 . 92 , 4 . 42 분 .