화합물 130 - E 1 LC / MS ESI 432 ( M + H ) + 1 H NMR ( 400 MHz , MeOD ) δ 7 . 59 - 7 . 56 ( m , 3 H ) , 7 . 39 ? 7 . 21 ( m , 5 H ) , 6 . 39 ( d , J = 7 . 3 Hz , 1 H ) , 4 . 97 ( s , 1 H ) , 4 . 44 ( s , 1 H ) , 3 . 44 ? 3 . 36 ( m , 4 H ) , 3 . 32 ? 3 . 15 ( m , 2 H ) , 2 . 81 - 2 . 79 ( m , 4 H ) , 2 . 71 ( t , J = 6 . 0 Hz , 2 H ) , 2 . 50 - 2 . 45 ( m , 1 H ) , 2 . 25 - 2 . 20 ( m , 1 H ) , 1 . 88 ? 1 . 85 ( m , 2 H ) . 키 랄 SFC B ( 40 % MeOH ) : ee 100 %, Rt = 1 . 34 분 .