화합물 130 - E 2 LC / MS ESI 432 ( M + H ) + 1 H NMR ( 400 MHz , MeOD ) δ 7 . 59 - 7 . 56 ( m , 3 H ) , 7 . 39 ? 7 . 21 ( m , 5 H ) , 6 . 39 ( d , J = 7 . 3 Hz , 1 H ) , 4 . 87 ( s , 1 H ) , 4 . 07 ( s , 1 H ) , 3 . 44 ? 3 . 26 ( m , 4 H ) , 2 . 92 ? 2 . 51 ( m , 8 H ) , 2 . 50 - 2 . 40 ( m , 1 H ) , 2 . 20 - 2 . 10 ( m , 1 H ) , 1 . 88 ? 1 . 85 ( m , 2 H ) . 키 랄 SFC B ( 40 % MeOH ) : ee 99 . 5 %, Rt = 2 . 89 분 .