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Norfolk -LRB- -LSB- ˈnɔərfɔərk -RSB- or -LSB- ˈnɔərfoʊk -RSB- -RRB- is a city in Madison County , Nebraska , United States , 113 miles northwest of Omaha and 83 miles west of Sioux City at the intersection of U.S. Routes 81 and 275 .. City. City. United States. United States. County. List of counties in Nebraska. Nebraska. Nebraska. Madison. Madison County, Nebraska. city. city. Madison County. Madison County, Nebraska. Omaha. Omaha, Nebraska. Sioux City. Sioux City, Iowa. U.S. Route 81. U.S. Route 275. The population was 24,210 at the 2010 census , making it the ninth-largest city in Nebraska .. Nebraska. Nebraska. 2010 United States Census. city. city. 2010 census. 2010 United States Census. ninth-largest city in Nebraska. List of cities in Nebraska. It is the principal city of the Norfolk Micropolitan Statistical Area .. city. city. Norfolk Micropolitan Statistical Area. Norfolk Micropolitan Statistical Area