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Valsartan and hydrochlorothiazide is manufactured by Novartis Pharmaceuticals. Valsartan and hydrochlorothiazide is a combination of two medicines -- valsartan and hydrochlorothiazide. Valsartan is a newer type of blood pressure medicine known as an angiotensin II receptor blocker, or ARB for short.
An efficient synthesis of the angiotensin-II inhibitor valsartan (Diovan Â®) is presented. Directed ortho-metalation of 5-phenyl-1-trityl-1 H-tetrazole (6) and its Negishi coupling with aryl bromide 5 are the key steps of the synthesis.he reaction mixture was heated to reflux at 75 Â°C for 2 h. The reaction was monitored by TLC until the starting material was consumed. Water (30 mL) was added to the reaction mixture and extracted with ethyl acetate (3 Ã 50 mL). The ethyl acetate layer was separated and concentrated under vacuum.